Title
Assignments of the paramagnetically shifted methyl resonances in the nuclear magnetic resonance spectrum of iron(III) protophyrin-IX cyanide by selective deuteriation
Document Type
Article
Publication Date
1-1-1974
Abstract
Synthese of 1,8- and 1,3-bis(trideuteriomethyl) protorphyrin-IX dimethyl esters [(1c) and (1d) respectively] are outlined, and these compounds, together with the 5,8-bis(trideuteriomethyl)isomer (1b) are used to specifically assign the paramagnetically shifted methyl resonances in the n.m.r. spectrum of iron(III) protoporphyrin-IX cyanide.
Publication Source (Journal or Book title)
Journal of the Chemical Society, Chemical Communications
First Page
392
Last Page
393
Recommended Citation
Cavaleiro, J., Rocha Gonsalves, A., Kenner, G., Smith, K., Shulman, R., Mayer, A., & Yamane, T. (1974). Assignments of the paramagnetically shifted methyl resonances in the nuclear magnetic resonance spectrum of iron(III) protophyrin-IX cyanide by selective deuteriation. Journal of the Chemical Society, Chemical Communications (10), 392-393. https://doi.org/10.1039/C39740000392